3,4,5-三甲氧基苯甲酸合成路线 （共 210 条）
反应条件
1: thionyl chloride 2: N-hydroxypyridine-2-thione sodium salt, AIBN, CH2I2 / toluene / 0.58 h / Heating View Scheme
参考文献
Barton, Derek H.R.; Lacher, Brigitte; Zard, Samir Z.
Tetrahedron, 1987 , vol. 43, # 19 p. 4321 - 4328
反应条件
2,2'-azo-bisisobutyronitrile; trichloromonobromomethane; 2,2’-disulfanediyldipyridine-1-oxide 2.) 100 deg C; Yield given. Multistep reaction;
参考文献
Barton, Derek H.R.; Lacher, Brigitte; Zard, Samir Z.
Tetrahedron Letters, 1985 , vol. 26, # 48 p. 5939 - 5942
反应条件
phosphorus pentachloride; benzene man leitet dann Ammoniak ein;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 340, p. 230
参考文献
Heffter; Capellmann
Chemische Berichte, 1905 , vol. 38, p. 3636
反应条件
1: thionyl chloride, DMF / toluene / 60 - 70 °C 2: 44 percent / tri-n-butylamine, palladium acetate / xylene / 2 h / 120 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 233, # 2 p. 267 - 274
反应条件
1: concentrated hydrochloric acid / im geschlossenen Rohr 2: HCl View Scheme
参考文献
Graebe; Martz
Chemische Berichte, 1903 , vol. 36, p. 216
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
参考文献
Harding
Journal of the Chemical Society, 1911 , vol. 99, p. 1593
Full Text Show Details
Thoms; Siebeling
Chemische Berichte, 1911 , vol. 44, p. 2116
反应条件
1: benzene; PCl5 / man leitet dann Ammoniak ein 2: hypochlorite; sodium hydroxide / unter Eiszusatz 3: Diazotization.Kochen der Loesung mit Schwefelsaeure View Scheme
参考文献
Qin, Qi-Xue; Yang, Jian; Chen, Duo-Zhi; Yang, Bo; Zhang, Ji
Organic Preparations and Procedures International, 2013 , vol. 45, # 4 p. 321 - 324
反应条件
sulfuric acid 50 h; Ambient temperature;
参考文献
Bao, Kai; Fan, Aixue; Dai, Yi; Zhang, Liang; Zhang, Weige; Cheng, Maosheng; Yao, Xinsheng
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 24 p. 5084 - 5090
