反应条件
1.1: n-BuLi; tetramethylethylendiamine / tetrahydrofuran; hexane / 1.5 h / -60 °C
1.2: 50 percent / tetrahydrofuran; hexane / 2.5 h / -60 - 20 °C
2.1: dimethylformamide / 0.75 h / 100 °C
3.1: sodium methanethiolate / dimethylformamide / 4 h / 100 - 140 °C
4.1: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C
View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
