1,7-二溴-3,4,9,10-苝四羧基双酐合成路线 （共 10 条）
反应条件
propionic acid T=140°C; 5 h;
参考文献
Kohl, Christopher; Weil, Tanja; Qu, Jianqiang; Muellen, Klaus
Chemistry - A European Journal, 2004 , vol. 10, # 21 p. 5297 - 5310
反应条件
1: With sulfuric acid
T=20°C; 2 h;
2: With bromine; iodine
T=80 - 100°C; 4 - 6 h;
参考文献
UNIVERSITA 'DEGLI STUDI DI ROMA "LA SAPIENZA"
Patent: WO2008/126123 A2, 2008 ;
Location in patent: Page/Page column 15; 19-20 ;
反应条件
sulfuric acid; bromine
T=40°C; 12 h;
参考文献
Zhou, Erjun; Tajima, Keisuke; Yang, Chunhe; Hashimoto, Kazuhito
Journal of Materials Chemistry, 2010 , vol. 20, # 12 p. 2362 - 2368
反应条件
potassium hydroxide in water; tert-butyl alcohol
T=90°C; 18 h;
参考文献
Chen, Zhijian; Baumeister, Ute; Tschierske, Carsten; Wuerthner, Frank
Chemistry - A European Journal, 2007 , vol. 13, # 2 p. 450 - 465
反应条件
sulfuric acid; bromine
T=85°C;
参考文献
Shaller, Andrew D.; Wang, Wei; Gan, Haiyang; Li, Alexander D. Q.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 40 p. 7705 - 7709
反应条件
1: With sulfuric acid; iodine
T=20°C; 2 h;
2: With bromine
T=80°C; 18 h;
参考文献
Choi, Jun; Sakong, Chun; Choi, Jae-Hong; Yoon, Chun; Kim, Jae Pil
Dyes and Pigments, 2011 , vol. 90, # 1 p. 82 - 88
反应条件
1: With sulfuric acid
T=20°C; 12 h;
2: With bromine; iodine
T=85 - 110°C; Title compound not separated from byproducts;
参考文献
Fan, Liqiang; Xu, Yanping; Tian, He
Tetrahedron Letters, 2005 , vol. 46, # 26 p. 4443 - 4447
反应条件
sulfuric acid; bromine; iodine
T=85°C; 24.5 h;
参考文献
Keerthi, Ashok; Valiyaveettil, Suresh
Journal of Physical Chemistry B, 2012 , vol. 116, # 15 p. 4603 - 4614
反应条件
sulfuric acid; bromine; iodine
T=85°C; 18 h;
参考文献
Naidu, Jaishri J.; Shin, Seunghan; Jeong, Kwang-Un; Lee, Myong-Hoon
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 9 p. 2705 - 2708
反应条件
sulfuric acid; bromine; iodine
参考文献
Nakatsuji, Shin'ichi; Aoki, Kazunori; Akutsu, Hiroki; Yamada, Jun-Ichi; Kojima, Takahiro; Nishida, Jun-Ichi; Yamashita, Yoshiro
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 9 p. 1079 - 1085
