1,2-溴-4,5-辛氧基苯合成路线 （共 8 条）
反应条件
sodium methylate in N,N-dimethyl-formamide Heating;
参考文献
Hanack, Michael; Guel, Ahmet; Hirsch, Andreas; Mandal, Braja K.; Subramanian, L. R.; Witke, Elisabeth
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 187, p. 365 - 382
反应条件
bromine in dichloromethane T=25°C; 2 h;
参考文献
Pol, J. F. van der; Neeleman, E.; Zwikker, J. W.; Nolte, R. J. M.; Drenth, W.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, p. 615 - 620
反应条件
1: K2CO3; KI / 10 h / Heating 2: Br2 / CH2Cl2 / 18 h / 0 - 20 °C View Scheme
参考文献
Pol, J. F. van der; Neeleman, E.; Zwikker, J. W.; Nolte, R. J. M.; Drenth, W.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, p. 615 - 620
反应条件
1: K2CO3; KI / 10 h / Heating 2: Br2 / CH2Cl2 / 18 h / 0 - 20 °C View Scheme
参考文献
Diaz Diaz, David; Torres, Tomas; Zentel, Rudolf; Davis, Riju; Brehmer, Martin
Chemical Communications, 2007 , # 23 p. 2369 - 2371
反应条件
1: 63 percent / K2CO3 / dimethylsulfoxide / 8 h / 100 °C 2: 88 percent / Br2 / CH2Cl2 / 2 h / 25 °C View Scheme
参考文献
Pol, J. F. van der; Neeleman, E.; Zwikker, J. W.; Nolte, R. J. M.; Drenth, W.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, p. 615 - 620
反应条件
1: 63 percent / dimethylformamide / 5 h / Heating 2: Na, NH3 (gas) / 1.) 1 h, r.t.; 2.) 4 h, 60 deg C View Scheme
参考文献
Sauer, Thomas; Wegner, Gerhard
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 162, p. 97 - 118
反应条件
in N,N-dimethyl-formamide 6 h; Heating;
参考文献
Pol, J. F. van der; Neeleman, E.; Zwikker, J. W.; Nolte, R. J. M.; Drenth, W.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, p. 615 - 620
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Hanack, Michael; Guel, Ahmet; Hirsch, Andreas; Mandal, Braja K.; Subramanian, L. R.; Witke, Elisabeth
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 187, p. 365 - 382
