反应条件
1: 1.) zinc chloride; 2.) diisobutylsluminum hydride (DIBAL) / 1.) THF, 30 min, room temperature; 2.) THF, hexane,-90 deg C, 5 h 2: 1.) THF, 1 h, 0 deg C; 2.) 15 min 3: 74 percent / aluminum amalgam / tetrahydrofuran; H2O / 3 h / Ambient temperature View Scheme
参考文献
Fujitsawa, Tamotsu; Fujimura, Atsushi; Sato, Toshio
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 1273 - 1280
