1,3-二亚氨基-5,6-双(辛氧基)异吲哚啉合成路线 （共 6 条）
反应条件
1: 77 percent / K2CO3 / dimethylformamide / 5 h / 80 °C 2: 63 percent / dimethylformamide / 5 h / Heating 3: Na, NH3 (gas) / 1.) 1 h, r.t.; 2.) 4 h, 60 deg C View Scheme
参考文献
Sauer, Thomas; Wegner, Gerhard
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 162, p. 97 - 118
反应条件
1: 63 percent / dimethylformamide / 5 h / Heating 2: Na, NH3 (gas) / 1.) 1 h, r.t.; 2.) 4 h, 60 deg C View Scheme
参考文献
Sauer, Thomas; Wegner, Gerhard
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 162, p. 97 - 118
反应条件
1: 85.5 percent / Br2 / acetic acid / 5 h / 10 °C 2: 77 percent / K2CO3 / dimethylformamide / 5 h / 80 °C 3: 63 percent / dimethylformamide / 5 h / Heating 4: Na, NH3 (gas) / 1.) 1 h, r.t.; 2.) 4 h, 60 deg C View Scheme
参考文献
Sauer, Thomas; Wegner, Gerhard
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 162, p. 97 - 118
反应条件
ammonia; sodium 1.) 1 h, r.t.; 2.) 4 h, 60 deg C; Yield given;
参考文献
Sauer, Thomas; Wegner, Gerhard
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 162, p. 97 - 118
反应条件
quinoline; tetrachlorosilane T=190°C; 1 h;
参考文献
Sauer, Thomas; Wegner, Gerhard
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 162, p. 97 - 118
反应条件
quinoline; tetrachlorosilane T=190°C; 1 h;
参考文献
Sauer, Thomas; Wegner, Gerhard
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 162, p. 97 - 118
