1: (S)-methyl 2-((diphenylmethylene)amino)pent-4-enoate With hydrogenchloride; water in methanol
1 h; Reflux;
2: di-tert-butyl dicarbonate With sodium hydrogencarbonate in methanol; water
T=20°C; pH=8; 2 h;
参考文献
Mina, John G.; Mosely, Jackie A.; Ali, Hayder Z.; Denny, Paul W.; Steel, Patrick G.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 6 p. 1823 - 1830