(S)-2-Cbz-氨基丁烷-1,4-二醇合成路线 （共 6 条）
反应条件
diisobutylaluminium hydride in hexane; dichloromethane T=-95 - -93°C; 1 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 2 p. 123 - 138
反应条件
sodium tetrahydroborate in methanol Inert atmosphere;
参考文献
Garner, Philip; Weerasinghe, Laksiri; Van Houten, Ian; Hu, Jieyu
Chemical Communications, 2014 , vol. 50, # 38 p. 4908 - 4910
反应条件
sodium tetrahydroborate in tetrahydrofuran; methanol T=45 - 55°C;
参考文献
Tomori, Hiroshi; Shibutani, Kuniko; Ogura, Katsuyuki
Heterocycles, 1997 , vol. 44, # 1 p. 213 - 225
反应条件
boron trifluoride-tetrahydrofuran complex
参考文献
Journal of the Chemical Society - Series Chemical Communications, , # 23 p. 1792 - 1793
反应条件
triethylamine in ethyl acetate T=-20 - -5°C; 1 h;
参考文献
Tomori, Hiroshi; Shibutani, Kuniko; Ogura, Katsuyuki
Heterocycles, 1997 , vol. 44, # 1 p. 213 - 225
反应条件
1: 16.9 g / Et3N / ethyl acetate / 1 h / -20 - -5 °C 2: 2.60 g / 3 h / 40 °C 3: 92 percent / AcOH / 10percent Pd/C / H2O / 1.5 h / 100 °C View Scheme
参考文献
Tomori, Hiroshi; Shibutani, Kuniko; Ogura, Katsuyuki
Heterocycles, 1997 , vol. 44, # 1 p. 213 - 225
