1: With potassium acetate; palladium diacetate in N,N-dimethyl acetamide T=20°C; 0.0833333 h; Inert atmosphere; 2: With tetrabutyl ammonium fluoride; oxygen in N,N-dimethyl acetamide T=20 - 100°C;

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1.1: 1,1,1,3,3,3-hexamethyl-disilazane / dichloromethane / -12 - 20 °C / Inert atmosphere 2.1: diethylzinc / dichloromethane / 16 h / 0 °C / Inert atmosphere 3.1: potassium acetate; palladium diacetate / N,N-dimethyl acetamide / 0.08 h / 20 °C / Inert atmosphere 3.2: 20 - 100 °C View Scheme