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乙二醇
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63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
118286-24-1
合成路线
（共 8 条）
118286-24-1
→
反应条件
713134-72-6
(R)-二苯甲亚硫酰基乙酸甲酯
+
865811-65-0
(S)-莫达非尼羧酸酯甲酯
反应条件
1-n-butyl-3-methylimidazolium hexafluorophosphate in tetrachloromethane T=20°C; 48 h; Title compound not separated from byproducts.;
参考文献
Ternois, James; Guillen, Frederic; Plaquevent, Jean-Christophe; Coquerel, Gerard
Tetrahedron Asymmetry, 2007 , vol. 18, # 24 p. 2959 - 2964
118286-24-1
→
反应条件
68524-30-1
二苯甲基硫代乙酰胺
反应条件
ammonia in methanol T=15°C; 1 h;
参考文献
Cao, Jianjing; Prisinzano, Thomas E.; Okunola, Oluyomi M.; Kopajtic, Theresa; Shook, Matthew; Katz, Jonathan L.; Newman, Amy Hauck
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 48 - 52
118286-24-1
→
反应条件
112111-43-0
阿莫达非尼
反应条件
1: ammonium hydroxide; ammonium chloride / methanol / 72 h / 50 °C 2: dihydrogen peroxide; acetic acid / methanol; water / 24 h / 40 °C View Scheme
参考文献
Cao, Jianjing; Prisinzano, Thomas E.; Okunola, Oluyomi M.; Kopajtic, Theresa; Shook, Matthew; Katz, Jonathan L.; Newman, Amy Hauck
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 48 - 52
118286-24-1
→
反应条件
63547-25-1
(二苯甲基亚磺酰)乙酸甲酯
反应条件
dihydrogen peroxide in methanol; water T=30°C; Kinetics; Temperature;
参考文献
Yadav, Ganapati D.; Subramanian; Manyar, Haresh G.
Organic Process Research and Development, 2010 , vol. 14, # 3 p. 537 - 543
118286-24-1
→
反应条件
713134-72-6
(R)-二苯甲亚硫酰基乙酸甲酯
+
865811-65-0
(S)-莫达非尼羧酸酯甲酯
反应条件
1-n-butyl-3-methylimidazolium hexafluorophosphate in tetrachloromethane T=20°C; 48 h; Title compound not separated from byproducts.;
参考文献
Ternois, James; Guillen, Frederic; Plaquevent, Jean-Christophe; Coquerel, Gerard
Tetrahedron Asymmetry, 2007 , vol. 18, # 24 p. 2959 - 2964
118286-24-1
→
反应条件
112111-43-0
阿莫达非尼
反应条件
1: ammonium hydroxide; ammonium chloride / methanol / 72 h / 50 °C 2: dihydrogen peroxide; acetic acid / methanol; water / 24 h / 40 °C View Scheme
参考文献
Cao, Jianjing; Prisinzano, Thomas E.; Okunola, Oluyomi M.; Kopajtic, Theresa; Shook, Matthew; Katz, Jonathan L.; Newman, Amy Hauck
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 48 - 52
118286-24-1
→
反应条件
112111-43-0
阿莫达非尼
反应条件
1: ammonium hydroxide; ammonium chloride / methanol / 72 h / 50 °C 2: dihydrogen peroxide; acetic acid / methanol; water / 24 h / 40 °C View Scheme
参考文献
Cao, Jianjing; Prisinzano, Thomas E.; Okunola, Oluyomi M.; Kopajtic, Theresa; Shook, Matthew; Katz, Jonathan L.; Newman, Amy Hauck
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 48 - 52
118286-24-1
→
反应条件
112111-43-0
阿莫达非尼
反应条件
1: ammonium hydroxide; ammonium chloride / methanol / 72 h / 50 °C 2: dihydrogen peroxide; acetic acid / methanol; water / 24 h / 40 °C View Scheme
参考文献
Cao, Jianjing; Prisinzano, Thomas E.; Okunola, Oluyomi M.; Kopajtic, Theresa; Shook, Matthew; Katz, Jonathan L.; Newman, Amy Hauck
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 1 p. 48 - 52
