3-(4-甲氧基苯基)苯甲醛合成路线 （共 8 条）
反应条件
potassium phosphate; tetrabutylammomium bromide; palladium diacetate in ethanol T=20°C; Suzuki cross-coupling reaction; 2 h;
参考文献
Deng, Yijian; Gong, Liuzhu; Mi, Aiqiao; Liu, Hui; Jiang, Yaozhong
Synthesis, 2003 , # 3 p. 337 - 339
反应条件
lithium chloride; Palladacycle in various solvent(s) T=90°C; 5 h;
参考文献
Brody, Marcus S.; Finn
Tetrahedron Letters, 1999 , vol. 40, # 3 p. 415 - 418
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 0.0833333 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
反应条件
[PdCl2(bis(di-tert-butylphosphino)ferrocene)]; TPGS–750–M; triethylamine in water T=20°C; Inert atmosphere;
参考文献
Isley, Nicholas A.; Gallou, Fabrice; Lipshutz, Bruce H.
Journal of the American Chemical Society, 2013 , vol. 135, # 47 p. 17707 - 17710
反应条件
bis(triphenylphosphine)palladium(II)-chloride; lithium chloride in N,N-dimethyl-formamide 0.0333333 h; microwave irradiation;
参考文献
Larhed, Mats; Hoshino, Masahide; Hadida, Sabine; Curran, Dennis P.; Hallberg, Anders
Journal of Organic Chemistry, 1997 , vol. 62, # 16 p. 5583 - 5587
反应条件
1: With toluene-4-sulfonic acid in benzene 3 h; Reflux; 2: With chromium(VI) oxide; acetic acid in water T=10 - 20°C; 23 h;
参考文献
Helvetica Chimica Acta, , vol. 91, # 3 p. 559 - 568
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI 1.) benzene/THF, 63 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 20 p. 4844 - 4848
反应条件
1: With toluene-4-sulfonic acid in benzene 3 h; Reflux; 2: With oxygen in benzene 168 h; Mechanism;
参考文献
Helvetica Chimica Acta, , vol. 91, # 3 p. 559 - 568
