反应条件
in diethyl ether
addn. of 2,3-dimethyl-1,3-butadiene soln. to a soln. of HGeCl3 with stirring at room temp., stirring (1 h), filtn. of white solid, addn. of filtrate to a soln. of ethylmagnesium bromide under reflux, refluxing (3 h); hydrolizing with satd. NH4Cl soln., evapn. of solvent at room temp., chromy. (silica gel, hexane), GPC;
参考文献
Kobayashi, Masanori; Yoshida, Masato; Kobayashi, Michio
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3169 - 3174
