反应条件
1: phenylboronic acid neopentylglycol ester; pivalic acid sodium salt With silver carbonate; p-benozquinone; palladium diacetate in tert-butyl alcohol
T=120°C; 3 h;
2: With oxalyl dichloride in dichloromethane
T=0 - 20°C;
3: methanol With triethylamine in dichloromethane
T=0 - 20°C; 8 h; Further stages.;
参考文献
Giri, Ramesh; Maugel, Nathan; Li, Jiao-Jie; Wang, Dong-Hui; Breazzano, Steven P.; Saunders, Lindsey B.; Yu, Jin-Quan
Journal of the American Chemical Society, 2007 , vol. 129, # 12 p. 3510 - 3511
