3,4-二甲基己烷-3,4-二醇合成路线 (共 22 条)
反应条件
nickel oxide; aluminum oxide; hydrogen T=250 - 260°C; P=73550.8 Torr; Anfangsdruck;
参考文献
Schmerling; Friedman; Ipatieff
Journal of the American Chemical Society, 1940 , vol. 62, p. 2448
反应条件
T=250 - 260°C; P=73550.8 Torr; Hydrogenation;
参考文献
Schmerling; Friedman; Ipatieff
Journal of the American Chemical Society, 1940 , vol. 62, p. 2448
参考文献
Palmen
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 141, p. 113,119
反应条件
phosphoric acid; acetic anhydride T=160 - 170°C;
参考文献
Gostunskaja et al.
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 1448,1449,1450;engl.Ausg.S.1393,1394,1395
反应条件
T=300°C; Produkt 5: 3.3-Dimethyl-hexanon-(4);
参考文献
Kuwata
Nippon Kagaku Kaishi, 1941 , vol. 62, p. 1035,1037,1040
Chem.Abstr., 1947 , p. 3051
反应条件
2: triethyl phosphite / 100 h / Heating
View Scheme
参考文献
Quast, Helmut; Fuss, Andreas; Heublein, Alfred; Jakobi, Harald; Seiferling, Bernhard
Chemische Berichte, 1991 , vol. 124, # 11 p. 2545 - 2554
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
2: triethyl phosphite / 100 h / Heating
View Scheme
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reeve, Wilkins; Kuroda, Donna Reichel
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2305 - 2307
参考文献
Kuwata
Nippon Kagaku Kaishi, 1941 , vol. 62, p. 1035,1037,1040
Chem.Abstr., 1947 , p. 3051