3,4-二甲基己烷-3,4-二醇合成路线 （共 22 条）
反应条件
sulfuric acid
T=-40 - -10°C; 2 h; other reagents, solvents, times and temperatures; Product distribution;
参考文献
Martinelli, Michael J.; Khau, Vien V.; Horcher, Linus M.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5546 - 5547
反应条件
sulfuric acid; bromine
1.) -40 to -10 deg C, 1 h, 2.) MeOH, 0 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Martinelli, Michael J.; Khau, Vien V.; Horcher, Linus M.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5546 - 5547
参考文献
Nybergh
Chemische Berichte, 1922 , vol. 55, p. 1962
参考文献
Herschmann
Monatshefte fuer Chemie, 1893 , vol. 14, p. 238
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Pace
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1928 , vol. <6>8, p. 310
参考文献
Kuwata
Nippon Kagaku Kaishi, 1941 , vol. 62, p. 1035,1037,1040
Chem.Abstr., 1947 , p. 3051
反应条件
sulfuric acid
T=95 - 150°C;
参考文献
Nybergh
Chemische Berichte, 1922 , vol. 55, p. 1962
反应条件
sulfuric acid
T=-40 - -10°C; 2 h; other reagents, solvents, times and temperatures; Product distribution;
参考文献
Martinelli, Michael J.; Khau, Vien V.; Horcher, Linus M.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5546 - 5547
参考文献
Nybergh
Chemische Berichte, 1922 , vol. 55, p. 1962
反应条件
T=300°C; Produkt 5: 3.3-Dimethyl-hexanon-(4);
参考文献
Kuwata
Nippon Kagaku Kaishi, 1941 , vol. 62, p. 1035,1037,1040
Chem.Abstr., 1947 , p. 3051
参考文献
Kuwata
Nippon Kagaku Kaishi, 1941 , vol. 62, p. 1035,1037,1040
Chem.Abstr., 1947 , p. 3051
