2,2-二甲基-1-丁醇合成路线 (共 24 条)
反应条件
1: With trimethylamine in water T=75°C; 1 h; 2: With katalysator G gem WO 95/32171 in water T=125°C; P=30003 Torr; pH=5.3 - 8.3;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2004/92097 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C;
参考文献
Daw, Graham; Regan, Andrew C.; Watt, C. Ian F.; Wood, Evan
Journal of Physical Organic Chemistry, 2013 , vol. 26, # 12 p. 1048 - 1057
反应条件
DBTO Ambient temperatureIrradiation; Yield given. Yields of byproduct given;
参考文献
Suslick, Kenneth; Cook, Bruce; Fox, Mary
Journal of the Chemical Society, Chemical Communications, 1985 , # 9 p. 580 - 582
参考文献
Fessenden; Coon
Journal of medicinal chemistry, 1965 , vol. 8, # 5 p. 604 - 608
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Sarel; Newman
Journal of the American Chemical Society, 1956 , vol. 78, p. 5416,5418
参考文献
Conant; Webb; Mendum
Journal of the American Chemical Society, 1929 , vol. 51, p. 1253
反应条件
mercury 17 h; HeatingIrradiationother alkanes; selectivity of cross-dimerization, relative reactivities in cross-dimerizations; Product distributionMechanism;
参考文献
Brown, Stephen H.; Crabtree, Robert H.
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 2946 - 2953
反应条件
1: dichloromethane / 20 °C / |Cooling with ice 2: lithium aluminium tetrahydride / diethyl ether / 20 °C View Scheme
参考文献
Daw, Graham; Regan, Andrew C.; Watt, C. Ian F.; Wood, Evan
Journal of Physical Organic Chemistry, 2013 , vol. 26, # 12 p. 1048 - 1057
参考文献
Whitmore; Forster
Journal of the American Chemical Society, 1942 , vol. 64, p. 2967
参考文献
Faworski; Ssakara
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1920 , vol. 50, p. 56
Chem. Zentralbl., 1923 , vol. 94, # III p. 667