acetylacetone in diethyl ether byproducts: Et2NH, CO2; heating (2 h); distn. (vacuum); elem. anal.;

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in methanol Sn-complex and ligand were stirred in MeOH at room temp. for ca. 12 h; filtered, washed with EtOH, dried under vac. at 20°C for 10 h; elem. anal.;

in acetone soln. of ligand in acetone was added with stirring to soln. of Sn-complex in acetone, stirred for several h at room temp.; filtered, washed with EtOH, dried under vac. at 20°C for 10 h;