反应条件
1: (4-methoxyphenyl)methanol With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h; Inert atmosphere;
2: (S)-1-benzyl-2-[(E)-2-butenoyl]-5-phenyl-pyrazolidin-3-one in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
3: With water; ammonium chloride in tetrahydrofuran; hexane
T=20°C; Inert atmosphere; optical yield given as percent ee;
参考文献
Sibi, Mukund P.; Kawashima, Keisuke; Stanley, Levi M.
Organic Letters, 2009 , vol. 11, # 17 p. 3894 - 3897