二乙基(3-溴丙基)膦酸酯合成路线 (共 22 条)
反应条件
Substitution; Arbusov reaction; 1 h; Heating;
参考文献
Gali, Hariprasad; Karra, Srinivasa R.; Reddy, V. Sreenivasa; Katti, Kattesh V.
Angewandte Chemie - International Edition, 1999 , vol. 38, # 13-14 p. 2020 - 2023
反应条件
T=155 - 160°C; 0.5 h;
参考文献
Hassan, Jomaa
Patent: US6680308 B1, 2004 ;
Location in patent: Page column 13, 14 ;
反应条件
triethyl phosphite in nitrogen
反应条件
triethylamine in diethyl ether 2 h;
参考文献
Pudovik; Terent'eva; Kibardina
Russian Journal of General Chemistry, 2006 , vol. 76, # 5 p. 714 - 719
反应条件
in tetrahydrofuran 2 h; Heating;
参考文献
Brestkin, A. P.; Vikhreva, L. A.; Godovikov, N. N.; Garbatyuk, V. S.; Moralev, S. N.; Kabachnik, M. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 1900 - 1905
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 9 p. 2118 - 2123
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1511
参考文献
E-Journal of Chemistry, , vol. 9, # 3 p. 1320 - 1326
反应条件
(i) PCl3, O2, (ii) /BRN= 1718733/; Multistep reaction. Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 48, p. 484 - 487
反应条件
(i) PCl3, O2, (ii) /BRN= 1718733/; Multistep reaction. Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 48, p. 484 - 487
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene 1 h; Heating;
参考文献
Balczewski, Piotr; Pietrzykowski, Witold M.
Tetrahedron, 1996 , vol. 52, # 43 p. 13681 - 13694