4-苄氧基-3-氧代-丁腈合成路线 （共 2 条）
反应条件
sodium hydride in tetrahydrofuran; mineral oil T=20 - 50°C; 12 h; Inert atmosphere;
参考文献
BASF SE; MICHROWSKA-PIANOWSKA, Anna, Aleksandra; KORDES, Markus; HUTZLER, Johannes; NEWTON, Trevor, William; EVANS, Richard, Roger; KREUZ, Klaus; GROSSMANN, Klaus; SEITZ, Thomas; KLOET, Andree van der; WITSCHEL, Matthias; PARRA RAPADO, Liliana; LERCHL, Jens
Patent: WO2013/104561 A1, 2013 ;
Location in patent: Page/Page column 47 ;
反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / |Inert atmosphere 1.2: 12 h / 0 - 20 °C 2.1: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 20 - 50 °C / |Inert atmosphere View Scheme
参考文献
BASF SE; MICHROWSKA-PIANOWSKA, Anna, Aleksandra; KORDES, Markus; HUTZLER, Johannes; NEWTON, Trevor, William; EVANS, Richard, Roger; KREUZ, Klaus; GROSSMANN, Klaus; SEITZ, Thomas; KLOET, Andree van der; WITSCHEL, Matthias; PARRA RAPADO, Liliana; LERCHL, Jens
Patent: WO2013/104561 A1, 2013 ;
