4-溴甲基-3-甲氧基苯甲酸合成路线 （共 2 条）
反应条件
1: zinc dibromide / 1,4-dioxane / 14 h / 60 - 65 °C 2: 4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide / dichloromethane / 5 h / |Reflux 3: hydrogen / tetrahydrofuran / 2 h / 25 - 35 °C 4: 4-methyl-morpholine / dichloromethane / 0.5 h / 25 - 35 °C / |Inert atmosphere View Scheme
参考文献
Srinivas, Keesari; Srinivasan, Neti; Krishna, Muddasani Rama; Reddy, Chinta Raveendra; Arunagiri, Muthulingam; Lalitha, Routhu; Reddy, Kikkura Sri Rami; Reddy, Bijjula Sreenivasa; Reddy, Ghanta Mahesh; Reddy, Padi Pratap; Kumar, Muppa Kishore; Reddy, Manne Satyanaraya
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 952 - 954
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; 2,2'-azo-bisisobutyronitrile in chloroform
4 h; Reflux;
参考文献
Srinivas, Keesari; Srinivasan, Neti; Krishna, Muddasani Rama; Reddy, Chinta Raveendra; Arunagiri, Muthulingam; Lalitha, Routhu; Reddy, Kikkura Sri Rami; Reddy, Bijjula Sreenivasa; Reddy, Ghanta Mahesh; Reddy, Padi Pratap; Kumar, Muppa Kishore; Reddy, Manne Satyanaraya
Organic Process Research and Development, 2004 , vol. 8, # 6 p. 952 - 954
