alpha-溴-alpha-氰基乙酸乙酯合成路线 (共 15 条)
反应条件
bromine in tetrachloromethane T=100°C; 1 h; Irradiation;
参考文献
Yamada, Yoichi; Yasuda, Heinosuke
Synthesis, 1990 , # 9 p. 768 - 770
反应条件
carbon disulfide; bromine T=150°C;
参考文献
Thorpe; Young
Journal of the Chemical Society, 1900 , vol. 77, p. 941
Chem. News J. Ind. Sci., 1900 , vol. 81, p. 261
反应条件
tetrahydrofuran; dilithium tetrabromonickelate(II); water in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Khamliche, Layachi; Robert, Albert; Bakkas, Salem
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 1031 - 1034
反应条件
tetrahydrofuran; dilithium tetrabromonickelate(II); water in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Khamliche, Layachi; Robert, Albert; Bakkas, Salem
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 1031 - 1034
反应条件
tri-n-butyl-antimony 0.5 h; Ambient temperature;
参考文献
Chen, Chen; Liao, Yi; Huang, Yao-Zeng
Tetrahedron, 1989 , vol. 45, # 10 p. 3011 - 3020
参考文献
Zhurina,F.G.; Vul'fson,N.S.
Journal of Organic Chemistry USSR (English Translation), 1967 , vol. 3, p. 483 - 485
Zhurnal Organicheskoi Khimii, 1967 , vol. 3, p. 504 - 506
反应条件
acetic anhydride in N,N-dimethyl-formamide 12 h; Ambient temperature;
参考文献
Hamana, Masatomo; Fujimura, Yasuo; Nawata, Yoshiharu
Heterocycles, 1987 , vol. 25, p. 235 - 239
反应条件
tri-n-butyl-arsine T=80°C; 16 h;
参考文献
Shen, Yanchang; Yang, Baozhen
Synthetic Communications, 1989 , vol. 19, # 17 p. 3069 - 3076
反应条件
1: BrCH(CN)CO2Et; ethyl vinyl ether With MeOAMVN in dichloromethane T=25°C; Addition; 2 h; 2: ethanol in dichloromethane T=25°C; ethanolysis; 0.5 h;
参考文献
Kita, Yasuyuki; Sano, Atsunori; Yamaguchi, Takahiro; Oka, Masahisa; Gotanda, Kentoku; Matsugi, Masato
Journal of Organic Chemistry, 1999 , vol. 64, # 2 p. 675 - 678
反应条件
sodium ethanolate in diethyl ether Heating;
参考文献
Singh, Harjit; Ahuja, Amarjit S.; Malhotra, Nageshwar
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 653 - 656