1,3,5-三(4-氨苯基)苯合成路线 （共 10 条）
反应条件
palladium on activated charcoal; hydrogen in tetrahydrofuran T=20°C; P=9000.9 Torr; 3 h;
参考文献
Li, Guiyang; Wang, Zhonggang
Macromolecules, 2013 , vol. 46, # 8 p. 3058 - 3066
反应条件
tetrakis(triphenylphosphine) palladium(0); Aliquatreg; 336; potassium carbonate in water; toluene T=100°C; 24 h; Inert atmosphere;
参考文献
Schwab, Matthias Georg; Hamburger, Manuel; Feng, Xinliang; Shu, Jie; Spiess, Hans Wolfgang; Wang, Xinchen; Antonietti, Markus; Muellen, Klaus
Chemical Communications, 2010 , vol. 46, # 47 p. 8932 - 8934
反应条件
toluene-4-sulfonic acid in water T=142°C; 16 h; Neat (no solvent); chemoselective reaction;
参考文献
Zhao, Yanan; Li, Jian; Li, Chunju; Yin, Kun; Ye, Dongyan; Jia, Xueshun
Green Chemistry, 2010 , vol. 12, # 8 p. 1370 - 1372
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 2 h;
参考文献
Ishi-I, Tsutomu; Kuwahara, Rempei; Takata, Akihiko; Jeong, Yeonhwan; Sakurai, Kazuo; Mataka, Shuntaro
Chemistry - A European Journal, 2006 , vol. 12, # 3 p. 763 - 776
反应条件
1: SiCl4 / ethanol / 10 h / Heating 2: 5.6 g / NH2NH2*H2O / Pd/C / ethanol / 10 h / Heating View Scheme
参考文献
Xu, Wen-Zhi; Huang, Zhi-Tang; Zheng, Qi-Yu
Tetrahedron Letters, 2008 , vol. 49, # 33 p. 4918 - 4921
反应条件
1: aq. Na2CO3 / [Pd(PPh3)4] / 1,2-dimethoxy-ethane / 18 h / Heating 2: 76 percent / TFA / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Ishi-I, Tsutomu; Kuwahara, Rempei; Takata, Akihiko; Jeong, Yeonhwan; Sakurai, Kazuo; Mataka, Shuntaro
Chemistry - A European Journal, 2006 , vol. 12, # 3 p. 763 - 776
反应条件
1: 10 percent / aq. Na2CO3 / [Pd(PPh3)4] / 1,2-dimethoxy-ethane / 36 h / Heating 2: 76 percent / TFA / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Ishi-I, Tsutomu; Kuwahara, Rempei; Takata, Akihiko; Jeong, Yeonhwan; Sakurai, Kazuo; Mataka, Shuntaro
Chemistry - A European Journal, 2006 , vol. 12, # 3 p. 763 - 776
反应条件
arachno-[(η5-C5Me5RuCO)2B2H6] in toluene T=75°C; 40 h; Inert atmosphere;
参考文献
Geetharani; Tussupbayev, Samat; Borowka, Julia; Holthausen, Max C.; Ghosh, Sundargopal
Chemistry - A European Journal, 2012 , vol. 18, # 27 p. 8482 - 8489
反应条件
hydrogenchloride; hypophosphorous acid; sodium nitrite 1.) 0 deg C;
参考文献
Bonvoisin, Jacques; Launay, Jean-Pierre; Verbouwe, Wouter; Auweraer, Mark Van der; Schryver, Frans Carl De
Journal of Physical Chemistry, 1996 , vol. 100, # 42 p. 17079 - 17082
反应条件
hydrogenchloride; hypophosphorous acid; sodium nitrite 1.) 0 deg C;
参考文献
Bonvoisin, Jacques; Launay, Jean-Pierre; Verbouwe, Wouter; Auweraer, Mark Van der; Schryver, Frans Carl De
Journal of Physical Chemistry, 1996 , vol. 100, # 42 p. 17079 - 17082
