反应条件
bis(acetylacetonate)nickel(II); triethylaluminum; triphenylphosphine in neat (no solvent) molar ratio in catalytic system: Ni(acac)2:TPP:Al-compound 1:2:2, HGeEt3 ratio 2, in an steel autoclave under Ar, maintained for 72 h at 24°C; distilled under vacuo; total yield: 70.5percent;
参考文献
Salimgareeva, I. M.; Bogatova, N. G.; Panasenko, A. A.; Khalilov, L. M.; Purlei, I. I.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, p. 1456 - 1461
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , vol. 32, p. 1605 - 1612
