N,N-二甲基甲酰胺二乙基缩醛合成路线 （共 152 条）
参考文献
Robev, Stefan K.
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4351 - 4354
反应条件
1: N-(benzoyl)glycine With caesium carbonate; Merrifield resin in N,N-dimethyl-formamide
T=200°C; 0.166667 h;
2: 1,1-diethoxy-N,N-dimethylmethanamine in N,N-dimethyl-formamide
T=180°C; 0.166667 h;
3: 2-aminopyridine With acetic acid
T=180°C; 0.166667 h; microwave irradiation;
参考文献
Westman, Jacob; Lundin, Ronny
Synthesis, 2003 , # 7 p. 1025 - 1030
反应条件
T=85°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Dozorova, E. N.; Grizik, S. I.; Granik, V. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 1 p. 70 - 73
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , # 1 p. 81 - 84
参考文献
Bredereck,H. et al.
Chemische Berichte, 1964 , vol. 97, p. 61 - 73
参考文献
Bredereck,H. et al.
Chemische Berichte, 1964 , vol. 97, p. 61 - 73
反应条件
in tetrahydrofuran
T=55°C; 3 h;
参考文献
Okubo, Masao; Omote, Yasumasa
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 4 p. 212 - 220
反应条件
in tetrahydrofuran
T=55°C; 3 h;
参考文献
Okubo, Masao; Omote, Yasumasa
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 4 p. 212 - 220
反应条件
in dichloromethane
Ambient temperature;
参考文献
Gokou, Celestin Tea; Chehna, Moustafa; Pradere, Jean-Paul; Duguay, Guy; Toupet, Loic
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 327 - 340
反应条件
hydroxylamine-o-sulphonic acid
1.) 4 h, reflux, 2.) methanol, 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Isomura; Sakamoto; Ito; Homma; Abe; Kubo
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 152 - 165
反应条件
in toluene
2 h; Heating;
参考文献
Marchenko, N. B.; Granik, V. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , p. 1050 - 1052
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 10 p. 1321 - 1324
