N,N-二甲基甲酰胺二乙基缩醛合成路线 （共 152 条）
反应条件
in toluene 4 h; Heating;
参考文献
Guss, L. T.; Ershov, L. V.; Bogdanova, G. A.; Granik, V. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 2 p. 183 - 188
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , vol. 26, # 2 p. 215 - 220
反应条件
in ethanol 3.5 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 2 p. 183 - 188
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 2 p. 215 - 220
反应条件
in tetrahydrofuran T=55°C; 3 h;
参考文献
Okubo, Masao; Omote, Yasumasa
Journal of Physical Organic Chemistry, 1996 , vol. 9, # 4 p. 212 - 220
反应条件
1: N-(benzoyl)glycine With caesium carbonate; Merrifield resin in N,N-dimethyl-formamide T=200°C; 0.166667 h; 2: 1,1-diethoxy-N,N-dimethylmethanamine in N,N-dimethyl-formamide T=180°C; 0.166667 h; 3: 2-cyanomethyl pyridine With acetic acid T=180°C; 0.166667 h; microwave irradiation;
参考文献
Westman, Jacob; Lundin, Ronny
Synthesis, 2003 , # 7 p. 1025 - 1030
反应条件
iodine in diethyl ether 2 h; Heating; Product distribution;
参考文献
Kantlehner, Willi; Hauber, Michael; Haug, Erwin; Schallenmueller, Claus; Regele, Claudia
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 2000 , vol. 342, # 7 p. 682 - 699
参考文献
Meerwein,H. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 641, p. 1 - 39
反应条件
hydrogen; nickel 1) DMF, reflux, 10 min, 2) THF-CH3OH, atm. pressure, 2.5 h; Yield given. Multistep reaction;
参考文献
Baberkina, E. P.; Akhvlediani, R. N.; Buyanov, V. N.; Kuleshova, E. F.; Suvorov, N. N.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 11 p. 2201 - 2203
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 11 p. 2440 - 2442
反应条件
iodine in diethyl ether 2 h; Heating; Product distribution;
参考文献
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), , vol. 342, # 7 p. 682 - 699
参考文献
Meerwein,H. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 641, p. 1 - 39
参考文献
Moffat, David; Davis, Peter; Hutchings, Martin; Davis, Jeremy; Berg, Daniel; Batchelor, Mark; Johnson, James; O'Connell, James; Martin, Richard; Crabbe, Tom; Delgado, Jean; Perry, Martin
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 23 p. 3351 - 3356
