N,N-二甲基甲酰胺二乙基缩醛合成路线 （共 152 条）
参考文献
Bredereck,H. et al.
Chemische Berichte, 1964 , vol. 97, p. 3397 - 3406
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Meerwein,H. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 641, p. 1 - 39
参考文献
Wagner,R.M.; Jutz,C.
Chemische Berichte, 1971 , vol. 104, p. 2975 - 2983
反应条件
in diethyl ether T=20°C; 2 h;
参考文献
Obschestvo S Ogranichennoi Otvetstvennostju "Unikorm"; GRANIK, Vladimir Grigorevich; PARSHIN, Valery Aleksandrovich; GOLOVKO, Tatyana Vasilyevna; TUGUSHEVA, Nelya Zarifovna; MEDVEDEVA, Marina Igorevna
Patent: EP2564851 A2, 2013 ;
Location in patent: Paragraph 0014-0015 ;
反应条件
in N,N-dimethyl-formamide T=80°C; 24 h;
参考文献
Gilley, Cynthia B.; Buller, Matthew J.; Kobayashi, Yoshihisa
Organic Letters, 2007 , vol. 9, # 18 p. 3631 - 3634
反应条件
nitrogen in N,N-dimethyl-formamide
参考文献
Hoffmann-La Roche Inc.
Patent: US3976639 A1, 1976 ;
反应条件
in N,N-dimethyl-formamide T=150°C; 16 h;
参考文献
Nathubhai, Amit; Patterson, Richard; Woodman, Timothy J.; Sharp, Harriet E. C.; Chui, Miranda T. Y.; Chung, Hugo H. K.; Lau, Stephanie W. S.; Zheng, Jun; Lloyd, Matthew D.; Thompson, Andrew S.; Threadgill, Michael D.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 17 p. 6089 - 6099
反应条件
in DMF (N,N-dimethyl-formamide) T=140°C; 52 h;
参考文献
CELLTECH R and D LIMITED
Patent: WO2004/7428 A1, 2004 ;
Location in patent: Page 43 ;
参考文献
Palacios, Francisco; Aparicio, Domitila; Vicario, Javier
European Journal of Organic Chemistry, 2002 , # 24 p. 4131 - 4136
反应条件
in methanol 5 h; Ambient temperature;
参考文献
Koelle, Ulrich; Kolb, Bernd; Mannschreck, Albrecht
Chemische Berichte, 1980 , vol. 113, # 7 p. 2545 - 2565
反应条件
hydrogenchloride in ethanol 1) 20-25 Deg C, 1 h, 2) 80 deg C, 45 min.;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 3 p. 613 - 617
Zhurnal Organicheskoi Khimii, , vol. 20, # 3 p. 673 - 678
