N,N-二甲基甲酰胺二乙基缩醛合成路线 (共 152 条)
反应条件
in ethanol T=20 - 25°C; 1 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 3 p. 613 - 617
Zhurnal Organicheskoi Khimii, , vol. 20, # 3 p. 673 - 678
参考文献
Justus Liebigs Annalen der Chemie, , vol. 641, p. 1 - 39
反应条件
in ethanol 5 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 20, # 9 p. 1026 - 1031
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 20, # 9 p. 1252 - 1256
反应条件
iodine in diethyl ether 2 h; Heating; Product distribution;
参考文献
Kantlehner, Willi; Hauber, Michael; Haug, Erwin; Schallenmueller, Claus; Regele, Claudia
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 2000 , vol. 342, # 7 p. 682 - 699
反应条件
in acetic acid; N,N-dimethyl-formamide
参考文献
Meerwein,H. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 641, p. 1 - 39
参考文献
McBride, L. J.; Caruthers, M. N.
Tetrahedron Letters, 1983 , vol. 24, # 29 p. 2953 - 2956
反应条件
in N,N-dimethyl-formamide 6 h; Heating;
参考文献
Damewood Jr.; Edwards; Feeney; Gomes; Steelman; Tuthill; Williams; Warner; Woolson; Wolanin; Veale
Journal of Medicinal Chemistry, 1994 , vol. 37, # 20 p. 3303 - 3312
参考文献
Brechbuehler,H. et al.
Angewandte Chemie, 1963 , vol. 75, p. 296
反应条件
sodium hydroxide; ammonium formate; palladium in ethanol; water; N,N-dimethyl-formamide; toluene; benzene
参考文献
Boehringer Ingelheim Pharmaceuticals, Inc.
Patent: US2003/162968 A1, 2003 ;
参考文献
Lee, Ka Young; Lee, Mi Jung; GowriSankar, Saravanan; Kim, Jae Nyoung
Tetrahedron Letters, 2004 , vol. 45, # 26 p. 5043 - 5046