反应条件
Multi-step reaction with 3 steps 1: 69 percent / HCl gas / CHCl3 / 1 h / 0 °C2: 1.) BuLi / 1.) THF, - 78 deg C, 30 min; 2.) THF, -78 deg C, 90 min; 3.) THF, -78 deg C, 2 h3: 30 percent / mercury(II) trifluoroacetate / tetrahydrofuran / 48 h / Ambient temperature
参考文献
Pelter, Andrew; Ward, Robert S.; Pritchard, Martyn C.; Kay, I. Trevor Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1603 - 1614
