1: diethyl ether / 7 h / Heating 2: LAH / diethyl ether / 6 h / Heating 3: 2.) H2 / 2.) 10percent Pd-C / 1.) MeOH, 14 h, 2.) 50 deg C, 760 torr, 7 h View Scheme

1: LAH / diethyl ether / 6 h / Heating 2: 2.) H2 / 2.) 10percent Pd-C / 1.) MeOH, 14 h, 2.) 50 deg C, 760 torr, 7 h View Scheme

hydrogen; palladium on activated charcoal 1.) MeOH, 14 h, 2.) 50 deg C, 760 torr, 7 h; Yield given. Multistep reaction;