4,4',4''-三羧基三苯胺合成路线 （共 3 条）
反应条件
bromine; sodium hydroxide in 1,4-dioxane; water T=45°C; 5 h;
参考文献
Wang, Jian; He, Cheng; Wu, Pengyan; Wang, Jing; Duan, Chunying
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12402 - 12405
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 12 h / 20 °C 2: bromine; sodium hydroxide / 1,4-dioxane; water / 5 h / 45 °C View Scheme
参考文献
Wang, Jian; He, Cheng; Wu, Pengyan; Wang, Jing; Duan, Chunying
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12402 - 12405
反应条件
n-butyllithium 1.) 0 deg C, 30 min, 2.) r. t., 30 min, sonication;
参考文献
Dapperheld, Steffen; Steckhan, Eberhard; Grosse Brinkhaus, Karl-Heinz; Esch, Thomas
Chemische Berichte, 1991 , vol. 124, # 11 p. 2557 - 2568
