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1: LiCl, CuCl*2H2O / H2O; acetone / 1.) 2 h, 3 to 10 deg C, 2.) 2 h, 10 deg C to room temp., 3.) 2 h, room temp. 2: Fe, HOAc, sodium acetate dihydrate / ethanol; H2O / 2 h / Heating View Scheme