反应条件
in 1,4-dioxane; water ligand refluxed with P2S5 for 10 h, filtered while hot, aq. soln. of NiCl2 added (10:15:4.9 molar ratio), refluxed for 2-4 h; crystd. on cooling, crystd., filtered off, washed (dioxane, H2O, EtOH, ether), dried, recrystd. (DCM), elem. anal.;
参考文献
Miao, Qingqing; Gao, Junxiong; Wang, Zeqing; Yu, Hang; Luo, Yi; Ma, Tingli
Inorganica Chimica Acta, 2011 , vol. 376, # 1 p. 619 - 627