反应条件
1.1: hydrazine hydrate; acetic acid / ethanol / |Reflux
2.1: magnesium sulfate; manganese(IV) oxide / dichloromethane / 0 - 20 °C
3.1: copper(l) iodide; cesium fluoride / 1-methyl-pyrrolidin-2-one / 0.5 h / 20 °C / |Glovebox; |Schlenk technique
3.2: 0.08 h / |Glovebox; |Schlenk technique
View Scheme
参考文献
Hu, Mingyou; He, Zhengbiao; Gao, Bing; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17302 - 17305