molecular sieve; tris(dimethylamino)-sulphonium difluorotrimethylsilicate in tetrahydrofuran T=20°C; 1 h;
参考文献
Palomo, Claudio; Aizpurua, Jesus M.; Garcia, Jesus M.; Ganboa, Inaki; Cossio, F. P.; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2498 - 2503
Adams, Dave J.; Clark, James H.; Hansen, Liv B.; Sanders, Victoria C.; Tavener, Stewart J.
Journal of Fluorine Chemistry, 1998 , vol. 92, # 2 p. 123 - 125
potassium hydroxide; tetra-(n-butyl)ammonium iodide in water Heatingother temperature; various phase transfer catalysts; condensation of diaryl ketones with acetonitrile in the presence of KOH; temperature dependence; effect of water, phase transfer catalysts, cosolvent; kinetics and mechanism; Rate constantProduct distribution;
参考文献
Bentley, T. William; Jones, Ray V. H.; Larder, Annette H.; Lock, Stephen J.
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 1 p. 89 - 94
potassium hydroxide; water T=82 - 83°C; time dependence, effect of Ph2CO and H2O amounts, effect of quaternary ammonium salts and cosolvents additions, also at 84 deg C; Rate constantProduct distribution;
参考文献
Bentley, T. William; Jones, Ray V.H.; Larder, Annette H.; Lock, Stephen J.
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 6 p. 1407 - 1411
Gilman, H.; Rosenberg, S. D.
Journal of Organic Chemistry, 1953 , vol. 18, p. 1554 - 1560
Full Text View citing articles Show Details
Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.16.1.1, page 141 - 147