2-氨基-1-(4-硝基苯基)-1,3-丙二醇合成路线 (共 90 条)
反应条件
1: palladium / Hydrogenation 2: pyridine 3: amidosulfuric acid; nitric acid 4: aqueous hydrochloric acid 5: Gewinnung ueber das (1S)-2-Oxo-bornan-sulfonat-(10) View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2463
反应条件
2: pyridine 3: amidosulfuric acid; nitric acid 4: aqueous hydrochloric acid 5: Gewinnung ueber das (1S)-2-Oxo-bornan-sulfonat-(10) View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2463
反应条件
1: amidosulfuric acid; nitric acid 2: aqueous hydrochloric acid 3: Gewinnung ueber das (1S)-2-Oxo-bornan-sulfonat-(10) View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2463
反应条件
1: aqueous hydrochloric acid 2: Gewinnung ueber das (1S)-2-Oxo-bornan-sulfonat-(10) View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2463
反应条件
1: pyridine 2: palladium / Hydrogenation 3: pyridine 4: amidosulfuric acid; nitric acid 5: aqueous hydrochloric acid 6: Gewinnung ueber das (1S)-2-Oxo-bornan-sulfonat-(10) View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 2463
反应条件
sodium tetrahydroborate in methanol T=60°C; Inert atmosphere;
参考文献
Li, Qiong; Zhang, Hongbo; Li, Chenguang; Xu, Pengfei
Chinese Journal of Chemistry, 2013 , vol. 31, # 1 p. 149 - 153
反应条件
hydrogenchloride T=90°C; Yield given;
参考文献
Tetrahedron Letters, , vol. 39, # 46 p. 8503 - 8004
反应条件
1.1: Bu2SnO / 1,2-dichloro-ethane / 24 h / Heating 1.2: 6 h / Heating 1.3: 62 percent / Bu4NBr / 6 h / Heating 2.1: 80 percent / Ti(OiPr)4 / ethanol 3.1: 92 percent / NaBH4 4.1: 92 percent / NaOH View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 29 p. 5553 - 5556
反应条件
(1R,3R,4R,5R)-(-)-quinic acid
参考文献
Farmaco, Edizione Scientifica, , vol. 8, p. 41,46
反应条件
1.1: 98 percent / AD-mix-β 2.1: Bu2SnO / 1,2-dichloro-ethane / 24 h / Heating 2.2: 6 h / Heating 2.3: 62 percent / Bu4NBr / 6 h / Heating 3.1: 80 percent / Ti(OiPr)4 / ethanol 4.1: 92 percent / NaBH4 5.1: 92 percent / NaOH View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 29 p. 5553 - 5556