1,2,3,4-四氢萘合成路线 (共 818 条)
反应条件
CoCl2.6H2O; lithium in tetrahydrofuran T=25°C; Birch reaction; 15 h; Inert atmosphere; regioselective reaction;
参考文献
Nador, Fabiana; Moglie, Yanina; Vitale, Cristian; Yus, Miguel; Alonso, Francisco; Radivoy, Gabriel
Tetrahedron, 2010 , vol. 66, # 24 p. 4318 - 4325
反应条件
indium tribromide; 1,1,3,3-tetramethyldisiloxane; iodine in chloroform T=20 - 60°C; 0.583333 h; Sealed tubeInert atmosphere;
参考文献
Moriya, Toshimitsu; Yoneda, Shinichiro; Kawana, Keita; Ikeda, Reiko; Konakahara, Takeo; Sakai, Norio
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10642 - 10650
反应条件
trifluoroacetic acid in tetrahydrofuran T=-20°C; 4 h; Irradiationquartz NMR tube; low-pressure mercury lamp(254 nm); var.: MeOH; Yield given;
参考文献
Journal of the American Chemical Society, , vol. 109, # 8 p. 2471 - 2475
反应条件
ethanol; nickel T=200°C; P=73550.8 - 147102 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 60, p. 664,666
反应条件
ammonium hydroxide in methanol T=10°C; 6 h; Irradiation; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 113, # 7 p. 2709 - 2717
反应条件
trifluorormethanesulfonic acid; silica gel in tetrachloromethane T=77°C; 4 h;
参考文献
Kropp, Paul J.; Breton, Gary W.; Craig, Stephen L.; Crawford, Scott D.; Durland, William F.; et al.
Journal of Organic Chemistry, 1995 , vol. 60, # 13 p. 4146 - 4152
反应条件
triethylsilane; tris(pentafluorophenyl)-borane in dichloromethane T=20°C;
参考文献
Synthesis, , # 2 p. 308 - 311
反应条件
hydrogen; palladium on activated charcoal in various solvent(s) T=109.85°C; P=3750.3 Torr; 1 h;
参考文献
Chemistry Letters, , vol. 35, # 7 p. 780 - 781
反应条件
sodium tetrahydroborate; NiII chloride hexahydrate in tetrahydrofuran; methanol T=20°C; 0.416667 h;
参考文献
Khurana, Jitender M.; Magoo, Devanshi
Synthetic Communications, 2010 , vol. 40, # 19 p. 2908 - 2913
反应条件
ammonium hydroxide in methanol T=10°C; 2.5 h; Irradiation; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 113, # 7 p. 2709 - 2717