1,2,3,4-四氢萘合成路线 （共 818 条）
反应条件
iodosylbenzene; (salen)manganese(III) complex (C104H90MnN2O2Si2(1+)*PF6(1-)) in chlorobenzene T=-20°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Churakova, Ekaterina; Kluge, Martin; Ullrich, Rene; Arends, Isabel; Hofrichter, Martin; Hollmann, Frank
Angewandte Chemie - International Edition, 2011 , vol. 50, # 45 p. 10716 - 10719
反应条件
pseudomonas monteilii TA-5 monooxygenase; tris(hydroxymethyl)methylamine hydrochloride in methanol T=30°C; pH=7; 0.25 h; aq. bufferEnzymatic reaction;
参考文献
Zhang, Wei; Tang, Weng Lin; Wang, Daniel I. C.; Li, Zhi
Chemical Communications, 2011 , vol. 47, # 11 p. 3284 - 3286
反应条件
1: AlCl3 / benzene 2: N2H4*H2O, KOH / bis-(2-hydroxy-ethyl) ether / Heating 3: H2SO4 4: Pd-C / Heating 5: (saponification) 6: (i) SOCl2, Py, Et2O, (ii) SnCl4, benzene View Scheme
参考文献
Chirico, R. D.; Hossenlopp, I. A.; Nguyen, A.; Steele, W. V.; Gammon, B. E.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 2 p. 179 - 202
反应条件
1: (i) AlCl3, (ii) /BRN= 1718733/, HCl 2: sulfur / 190 - 205 °C 3: (reduction) 4: H2SO4 5: (i) (reduction), (ii) Se (heating) View Scheme
参考文献
Tatta,K.R.; Bardhan,J.C.
Journal of the Chemical Society [Section] C: Organic, 1968 , vol. <C>, p. 893 - 900
参考文献
Kindler; Peschke
Justus Liebigs Annalen der Chemie, 1933 , vol. 501, p. 191,198
反应条件
in 1,2,3,4-tetrahydro-naphthalene 207°C; Hoffman, C. J. , Inorg. Synth., 1963, 7, 180; HI vapor was passed through a tetralin trap before condensing in a N2 trap, low-temp. distillation in vac.;
参考文献
Gmelin Handbook: I: MVol.2, 8, page 262 - 263
Full Text Show Details
Boedler, J.
Patent: DE405376 , 1922 ;
参考文献
Robertson; Waters
Journal of the Chemical Society, 1948 , p. 1581,1585
Full Text Show Details
Medwedew; Podjapolsskaja
Zhurnal Fizicheskoi Khimii, 1939 , vol. 13, p. 719
Chem. Zentralbl., 1940 , vol. 111, # I p. 688
参考文献
v. Braun; Deutsch
Chemische Berichte, 1912 , vol. 45, p. 1268
参考文献
Akabori; Suzuki
Proceedings of the Imperial Academy (Tokyo), vol. 5, p. 255
Chem. Zentralbl., 1929 , vol. 100, # II p. 2033
反应条件
1: aluminium chloride / 50 - 70 °C 2: bei aufeinanderfolgender Oxydation mit sodaalkalischer und mit schwefelsaurer Permanganat-Loesung 3: 290 °C / 13 Torr View Scheme
参考文献
Chemische Berichte, , vol. 57, p. 2014
Chem. Zentralbl., , vol. 99, # II p. 1386
