1,2,3,4-四氢萘合成路线 (共 818 条)
反应条件
hydrogenchloride; aluminium trichloride in chlorobenzene T=20°C; 1 h;
参考文献
Frenzel, Ralf; Domschke, Guenter; Roessler, Ljuba; Mayer, Roland
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1993 , vol. 335, # 6 p. 558 - 560
反应条件
1: aluminium chloride; carbon disulfide 2: phosphorus pentachloride 3: ammonia View Scheme
参考文献
v. Braun; Kirschbaum; Schuhmann
Chemische Berichte, 1920 , vol. 53, p. 1165
反应条件
1: With AlCl3, aluminium chloride in Carbon disufide T=60°C; 16 h; 2: With hydrogenchloride in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; chloroform T=0°C;
参考文献
ASTRAZENECA AB
Patent: WO2004/792 A1, 2003 ;
Location in patent: Page 20 ;
反应条件
Behandlung des in Aether geloesten Reaktionsprodukts mit NaOH;
参考文献
Houben; Fischer
Chemische Berichte, 1933 , vol. 66, p. 339,344
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Houben
Chemische Berichte, 1930 , vol. 63, p. 2455,2461
反应条件
1: aqueous HCl / Einleiten von HCl 2: zinc dust; aq.-ethanolic HCl View Scheme
参考文献
Badger; Cook; Crosbie
Journal of the Chemical Society, 1947 , p. 1432
反应条件
aluminium trichloride in dichloromethane T=20°C; 3 h;
参考文献
Daukshas, V.K.; Gaidyalis, P.G.; Labanauskas, L.K.; Gumbaragite, L.F.; Gasperavichene G.A.
Pharmaceutical Chemistry Journal, 1991 , vol. 25, # 10 p. 716 - 718
Khimiko-Farmatsevticheskii Zhurnal, 1991 , vol. 25, # 10 p. 41 - 42
反应条件
1: bromine / hexane / |Reflux; |Inert atmosphere 2: sodium hydrogencarbonate; water / acetone / |Reflux; |Inert atmosphere 3: water / 24 h / 20 °C / |Inert atmosphere 4: methanol / -5 °C / |Inert atmosphere 5: potassium carbonate / water; dichloromethane View Scheme
参考文献
Draper, Richard W.; Hou, Donald
Organic Process Research and Development, 1998 , vol. 2, # 3 p. 175 - 185
参考文献
Arbusov; Abramov; Shapshinskaya
Doklady Akademii Nauk SSSR, 1945 , vol. 46, p. 147
反应条件
hydrogenchloride; phosphoric acid; acetic acid T=100°C;
参考文献
Horn Jensen, Eva; Nielsen, Per Halfdan
Heterocycles, 1995 , vol. 41, # 11 p. 2441 - 2458
反应条件
hydrogenchloride; formaldehyd; sulfuric acid T=60 - 65°C; Einleiten von HCl;
参考文献
Arnold; Barnes
Journal of the American Chemical Society, 1943 , vol. 65, p. 2393
Full Text View citing articles Show Details
Winthrop Chem. Co.
Patent: US1853083 , 1930 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE533132 , 1930 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 586
Full Text Show Details
I.G. Farbenind.
Patent: DE519807 , 1930 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 672