1,2,3,4-四氢萘合成路线 （共 818 条）
反应条件
styrene-4-vinyl(N-alkylpyridinium bromide) in water; acetic acid
T=23°C; 24 h;
参考文献
Zajc, Barbara; Zupan, Marko
Tetrahedron, 1989 , vol. 45, # 24 p. 7869 - 7878
反应条件
aluminium trichloride; chlorobenzene
Erhitzen des Reaktionsprodukts mit wss. Bromwasserstoffsaeure, Erwaermen der gebildeten Bromide mit Malonsaeure-diaethylester und Natriumaethylat in Aethanol. Erhitzen auf 220grad;
参考文献
Colonge; Rochas
Bulletin de la Societe Chimique de France, 1948 , p. 827
参考文献
Henze; Smith
Journal of the American Chemical Society, 1943 , vol. 65, p. 1090
反应条件
1: 1.) conc. HCl, conc. H2SO4, 2.) glacial AcOH, AcONa*3H2O, 3.) 4M NaOH, 4.) pyridinium dichromate, silica gel
2: 79 percent / sodium borohydride / ethanol / 1.5 h
3: 100 percent / SOCl2 / toluene / 2 h
4: dimethylsulfoxide / 3 h
5: 82 percent / 4M NaOH / 8 h / Heating
View Scheme
参考文献
Horn Jensen, Eva; Nielsen, Per Halfdan
Heterocycles, 1995 , vol. 41, # 11 p. 2441 - 2458
反应条件
1: AlCl3, EtNO2
2: H+, molecular sieves
3: H2 / Pd/C / acetic acid
View Scheme
参考文献
Dillenschneider,J.-P.; Maire,J.-C.
Bulletin de la Societe Chimique de France, 1964 , p. 2606 - 2609
参考文献
Colonge; Rochas
Bulletin de la Societe Chimique de France, 1948 , p. 827
反应条件
aluminium trichloride; nitrobenzene
参考文献
Krollpfeiffer; Schaefer
Chemische Berichte, 1923 , vol. 56, p. 630
反应条件
AlCl3, aluminium chloride in tetrachloroethane, 1,1,2,2-
T=20°C; Friedel-Crafts acylation; Cooling with ice;
参考文献
Zhang, Zhenfa; Sangaiah, Ramiah; Gold, Avram; Ball, Louise M.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5431 - 5435
反应条件
1: phosphorus pentoxide / 190 °C
3: 130 - 140 °C
View Scheme
参考文献
Schroeter
Chemische Berichte, 1924 , vol. 57, p. 2014
Chem. Zentralbl., 1928 , vol. 99, # II p. 1386
参考文献
Martin; Stoffyn
Bulletin des Societes Chimiques Belges, 1950 , vol. 59, p. 83,87
