1,2,3,4-四氢萘合成路线 （共 818 条）
反应条件
1: 68 percent / N,N-dichlorobenzenesulfonamide / CCl4 / 4.5 h / Heating
2: 90 percent / lead tetraacetate / acetic acid / 2 h / 30 - 50 °C
View Scheme
参考文献
Kremlev, M. M.; Moskalenko, A. I.; Bezverkhii, N. P.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1639 - 1640
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 9 p. 1924 - 1926
参考文献
Spaeth et al.
Chemische Berichte, 1930 , vol. 63, p. 134,136
参考文献
Brooke, Gerald M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 821 - 826
反应条件
(-)-chloro-lt;5,10,15,20-tetrakis(1,2,3,4,5,6,7,8-octahydro-1,4:5,8-dimethanoanthracene-9-yl)porphirinatogt;manganese(III); iodosylbenzene; t-BuPy in dichloromethane
0.666667 h; Product distribution;
参考文献
Halterman, Ronald L.; Jan, Shyi-Tai; Nimmons, Heather L.; Standlee, David J.; Khan, Masood A.
Tetrahedron, 1997 , vol. 53, # 33 p. 11257 - 11276
反应条件
Yield given. Multistep reaction;
参考文献
House, Herbert O.; Lee, Joseph H. C.; VanDerveer, Don; Wissinger, Jane E.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5285 - 5288
反应条件
T=110 - 130°C; unter Druck.Hydrogenation; Product distribution;
参考文献
v.Braun; Blessing; Zobel
Chemische Berichte, 1923 , vol. 56, p. 1990
Chemische Berichte, 1923 , vol. 56, p. 1999
Full Text Show Details
v.Braun; Zobel
Chemische Berichte, 1923 , vol. 56, p. 694
反应条件
1: 23 percent / ZnCl2 / 6 h / 75 - 110 °C
2: 20 percent / glacial AcOH, 85percent H3PO4, concd HCl / 6 h / Heating
3: 98 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating
4: 75 percent / sulfur / 1.58 h / 230 - 270 °C
View Scheme
参考文献
Jackson, Richard A.; Rhodes, Christopher J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 53 - 57
反应条件
p-Nitrobenzene sulphonamide; iodine in 1,2-dichloro-ethane
T=60°C; 2 h; Inert atmosphere;
参考文献
Baba, Haruka; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron Letters, 2011 , vol. 52, # 33 p. 4303 - 4307
反应条件
1: chlorosulfonic acid / -10 - -5 °C / und Kochen des entstandenen Chloridgemisches mit Wasser
2: durch Kalischmelze
3: sulfuric acid
View Scheme
参考文献
Schroeter
Justus Liebigs Annalen der Chemie, 1922 , vol. 426, p. 132
参考文献
Hurd; Webb
Journal of the American Chemical Society, 1936 , vol. 58, p. 2190,2193
