1,2,3,4-四氢萘合成路线 （共 818 条）
反应条件
SbF5; epoxysulfonyl fluoride
T=0°C; P=760 Torr; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tanaka, Mutsuo; Iyoda, Jun; Souma, Yoshie
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2677 - 2680
反应条件
hydrogenchloride; sodium hydroxide; dipyridinium dichromate; sulfuric acid; sodium acetate; silica gel; acetic acid
Yield given. Multistep reaction;
参考文献
Horn Jensen, Eva; Nielsen, Per Halfdan
Heterocycles, 1995 , vol. 41, # 11 p. 2441 - 2458
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iodine; hexacarbonyl chromium
1.) dibutyl ether, THF, 24 h, reflux, 2.) THF, -78 deg C, 1 h, 3.) THF, 0 deg C, 4 h, 4.) THF, -78 deg C, 5.) THF, 16 h, room temp.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cambie, Richard C.; Clark, George R.; Gallagher, Stewart R.; Rutledge, Peter S.; Stone, Martin J.; Woodgate, Paul D.
Journal of Organometallic Chemistry, 1988 , vol. 342, p. 315 - 338
反应条件
T=120°C; Hydrogenation;
参考文献
Riedel,J. D.
Patent: DE408665 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 466
反应条件
1: trifluoroacetic acid / dichloromethane / 18 h / 23 °C / |Inert atmosphere
2: N-ethyl-N,N-diisopropylamine; Cu(I)[(CH3CN)4]BF4 / dichloromethane; dimethyl sulfoxide / 2 h / 23 °C / |Inert atmosphere
View Scheme
参考文献
Sokolovs, Igors; Lubriks, Dmitrijs; Suna, Edgars
Journal of the American Chemical Society, 2014 , vol. 136, # 19 p. 6920 - 6928
参考文献
Buck et al.
Journal of the Institute of Petroleum, vol. 34, p. 353
Chem.Abstr., 1948 , p. 7012
反应条件
1: AlCl3; benzene
2: palladium coal / 270 °C
View Scheme
参考文献
Newman; Zahm
Journal of the American Chemical Society, 1943 , vol. 65, p. 1097,1099
反应条件
water; permanganate(VII) ion
T=65°C;
参考文献
Davies; Poole
Journal of the Chemical Society, 1928 , p. 1618
Full Text Show Details
v. Braun
Chemische Berichte, 1923 , vol. 56, p. 2338
Full Text Show Details
v. Braun, Tetralin-Ges.
Patent: DE405459 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 453
Full Text Show Details
Cornillot
Annales de Chimie (Cachan, France), 1927 , vol. <10> 7, p. 227,275
Annales de Chimie (Cachan, France), 1927 , vol. <10> 8, p. 120
参考文献
v. Braun
Chemische Berichte, 1923 , vol. 56, p. 2338
Full Text Show Details
v. Braun, Tetralin-Ges.
Patent: DE405459 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 453
Full Text Show Details
Cornillot
Annales de Chimie (Cachan, France), 1927 , vol. <10> 7, p. 227,275
Annales de Chimie (Cachan, France), 1927 , vol. <10> 8, p. 120
参考文献
Randall; Benger; Groocock
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, vol. 165, p. 1938> 432, 442
