反应条件
1.1: N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(I) bromide dimethylsulfide complex / tetrahydrofuran / 0.5 h / -55 °C 1.2: 2 h / -55 °C 2.1: hydroxylamine hydrochloride; sodium acetate / dichloromethane / 4 h / 20 °C 3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere 4.1: tetrakis(triphenylphosphine) palladium(0); triethylamine / N,N-dimethyl-formamide / 0.13 h / 80 °C / Inert atmosphere View Scheme
参考文献
Heterocycles, , vol. 85, # 2 p. 383 - 401