2-(4-甲氧基苯基)-1,2,3,4-四氢异喹啉-1-甲腈合成路线 （共 15 条）
反应条件
Food Red No. 105 in acetonitrile T=20°C; 30 h; Irradiation;
参考文献
Pan, Yuanhang; Wang, Shuai; Kee, Choon Wee; Dubuisson, Emilie; Yang, Yuanyong; Loh, Kian Ping; Tan, Choon-Hong
Green Chemistry, 2011 , vol. 13, # 12 p. 3341 - 3344
反应条件
C43H35F5N2OPd; oxygen; acetic acid in methanol; acetonitrile T=20°C; 1.5 h; Photolysis;
参考文献
Chow, Pui-Keong; To, Wai-Pong; Low, Kam-Hung; Che, Chi-Ming
Chemistry - An Asian Journal, 2014 , vol. 9, # 2 p. 534 - 545
反应条件
2,4,5,7-tetrabromofluorescein in N,N-dimethyl-formamide T=20°C; 10 h; Irradiation;
参考文献
Hari, Durga Prasad; Koenig, Burkhard
Organic Letters, 2011 , vol. 13, # 15 p. 3852 - 3855
反应条件
Titanium(IV) oxide; acetic acid in ethanol 40 h; Irradiation;
参考文献
Rueping, Magnus; Zoller, Jochen; Fabry, David C.; Poscharny, Konstantin; Koenigs, Rene M.; Weirich, Thomas E.; Mayer, Joachim
Chemistry - A European Journal, 2012 , vol. 18, # 12 p. 3478 - 3481
反应条件
1: copper(l) iodide; potassium phosphate / ethylene glycol; isopropyl alcohol / 24 h / 20 - 90 °C / Inert atmosphere 2: 2,4,5,7-tetrabromofluorescein / N,N-dimethyl-formamide / 10 h / 20 °C / Irradiation View Scheme
参考文献
Alagiri, Kaliyamoorthy; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 4 p. 835 - 842
反应条件
copper(l) iodide; trimethylsilylazide; 2,3-dicyano-5,6-dichloro-p-benzoquinone T=90°C; 12 h; Inert atmosphereMolecular sieveSchlenk technique; Catalytic behaviorMechanism; ConcentrationReagent/catalystSolventTemperature;
参考文献
Zhang, Gen; Ma, Yunxia; Cheng, Guangbin; Liu, Dabin; Wang, Rui
Organic Letters, 2014 , vol. 16, # 3 p. 656 - 659
反应条件
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / Reflux 1.2: Cooling with ice 2.1: formic acid / 0.17 h / 0 °C 2.2: 24 h / 0 - 50 °C 3.1: copper(l) iodide; potassium phosphate / ethylene glycol; isopropyl alcohol / 24 h / 90 °C / Inert atmosphere 4.1: MoVIO2(acetylacetone)2; oxygen / 17 h / 80 °C / 760.05 Torr / Neat (no solvent) View Scheme
参考文献
Alagiri, Kaliyamoorthy; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 4 p. 835 - 842
反应条件
1.1: ammonium acetate; acetic acid / 1.5 h / Reflux 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / Reflux 2.2: Cooling with ice 3.1: formic acid / 0.17 h / 0 °C 3.2: 24 h / 0 - 50 °C 4.1: copper(l) iodide; potassium phosphate / ethylene glycol; isopropyl alcohol / 24 h / 90 °C / Inert atmosphere 5.1: MoVIO2(acetylacetone)2; oxygen / 17 h / 80 °C / 760.05 Torr / Neat (no solvent) View Scheme
参考文献
Alagiri, Kaliyamoorthy; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 4 p. 835 - 842
反应条件
1.1: formic acid / 0.17 h / 0 °C 1.2: 24 h / 0 - 50 °C 2.1: copper(l) iodide; potassium phosphate / ethylene glycol; isopropyl alcohol / 24 h / 90 °C / Inert atmosphere 3.1: MoVIO2(acetylacetone)2; oxygen / 17 h / 80 °C / 760.05 Torr / Neat (no solvent) View Scheme
参考文献
Alagiri, Kaliyamoorthy; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 4 p. 835 - 842
反应条件
copper(l) iodide; trimethylsilylazide; 2,3-dicyano-5,6-dichloro-p-benzoquinone T=80°C; 12 h; Inert atmosphereMolecular sieveSchlenk technique; Catalytic behavior;
参考文献
Zhang, Gen; Ma, Yunxia; Cheng, Guangbin; Liu, Dabin; Wang, Rui
Organic Letters, 2014 , vol. 16, # 3 p. 656 - 659
