4-[2-[(3-乙基-4-甲基-2-氧代-3-吡咯琳)甲酰胺基]乙基]苯磺酰胺合成路线 （共 7 条）
反应条件
ammonia in water T=60°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4853 - 4855
反应条件
1: 15 percent / H2; Ac2O / Ra-Ni / 40 °C / 3800 Torr 2: 90 percent / Na2CO3; H2O / Heating 3: 65 percent / toluene / Heating 4: ClSO3H / 10 °C 5: NH3 / H2O / 4 h / 60 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4853 - 4855
反应条件
1: 80 percent / dimethylformamide / 0 - 5 °C 2: 15 percent / H2; Ac2O / Ra-Ni / 40 °C / 3800 Torr 3: 90 percent / Na2CO3; H2O / Heating 4: 65 percent / toluene / Heating 5: ClSO3H / 10 °C 6: NH3 / H2O / 4 h / 60 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4853 - 4855
反应条件
1: 65 percent / toluene / Heating 2: ClSO3H / 10 °C 3: NH3 / H2O / 4 h / 60 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4853 - 4855
反应条件
1: 90 percent / Na2CO3; H2O / Heating 2: 65 percent / toluene / Heating 3: ClSO3H / 10 °C 4: NH3 / H2O / 4 h / 60 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4853 - 4855
反应条件
1: ClSO3H / 10 °C 2: NH3 / H2O / 4 h / 60 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 44, # 26 p. 4853 - 4855
反应条件
1: 4-[2-(3-ethyl-4-methyl-2-carbonyl pyrrolidine-amido)-ethyl]benzene sulfonamide With potassium carbonate T=55 - 60°C; 1 h; Heating / reflux; 2: trans-4-methyl- cyclohexyl isocyanate in toluene 12 h; Heating / reflux;
参考文献
WO2006/103690 A1, ;
Page/Page column 7,16 ;
