反应条件
1: methanol; hexane; dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2: 3-chloro-benzenecarboperoxoic acid / ethylene glycol dimethyl ether / 22.5 h / 20 °C / Inert atmosphere 3: chloroformic acid ethyl ester; 1,1,1,3,3,3-hexamethyl-disilazane / tetrahydrofuran / 16 h / 50 °C / Inert atmosphere View Scheme
参考文献
Bengtsson, Christoffer; Blaho, Stefan; Saitton, David Blomberg; Brickmann, Kay; Broddefalk, Johan; Davidsson, Oejvind; Drmota, Tomas; Folmer, Rutger; Hallberg, Kenth; Hallen, Stefan; Hovland, Ragnar; Isin, Emre; Johannesson, Petra; Kull, Bengt; Larsson, Lars-Olof; Loefgren, Lars; Nilsson, Kristina E.; Noeske, Tobias; Oakes, Nick; Plowright, Alleyn T.; Schnecke, Volker; Sthlberg, Pernilla; Soerme, Pernilla; Wan, Hong; Wellner, Eric; Oester, Linda
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 10 p. 3039 - 3053