4-(苯基乙炔基)苯硼酸频哪醇酯合成路线 (共 3 条)
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine in tetrahydrofuran Inert atmosphereReflux;
参考文献
Iwanaga, Tetsuo; Ida, Hiroko; Takezaki, Makoto; Toyota, Shinji
Chemistry Letters, 2011 , vol. 40, # 9 p. 970 - 971
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; triethylamine T=20°C; Sonogashira coupling; 0.0833333 h; Inert atmosphere; 2: With copper(l) iodide Sonogashira coupling; Inert atmosphere;
参考文献
Briones, John F.; Davies, Huw M. L.
Organic Letters, 2011 , vol. 13, # 15 p. 3984 - 3987
反应条件
oxygen; copper diacetate in dimethyl sulfoxide
T=60°C; P=760.051 Torr; 16 h;
参考文献
Khan, Bilal A.; Buba, Annette E.; Goossen, Lukas J.
Chemistry - A European Journal, 2012 , vol. 18, # 6 p. 1577 - 1581