2-三氟甲基-3-香叶基-1,4-萘醌合成路线 （共 6 条）
反应条件
manganese(IV) oxide in dichloromethane Ambient temperature; Yield given;
参考文献
Taguchi, Takeo; Suda, Yoshimitsu; Hosoda, Akihiko; Kobayashi, Yoshiro
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5765 - 5766
反应条件
1: 1.) n-BuLi, 2.) CuI / 1.) THF, -40 deg C, 20 min; 2.) THF, -78 deg C, 2 h 2: 10percent HCl / tetrahydrofuran; propan-2-ol / Ambient temperature 3: MnO2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Taguchi, Takeo; Suda, Yoshimitsu; Hosoda, Akihiko; Kobayashi, Yoshiro
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5765 - 5766
反应条件
1: Zn, AcOH / tetrahydrofuran / 0.08 h / Ambient temperature 2: iPr2NEt / tetrahydrofuran / 12 h / Ambient temperature 3: 1.) n-BuLi, 2.) CuI / 1.) THF, -40 deg C, 20 min; 2.) THF, -78 deg C, 2 h 4: 10percent HCl / tetrahydrofuran; propan-2-ol / Ambient temperature 5: MnO2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Taguchi, Takeo; Suda, Yoshimitsu; Hosoda, Akihiko; Kobayashi, Yoshiro
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5765 - 5766
反应条件
1: iPr2NEt / tetrahydrofuran / 12 h / Ambient temperature 2: 1.) n-BuLi, 2.) CuI / 1.) THF, -40 deg C, 20 min; 2.) THF, -78 deg C, 2 h 3: 10percent HCl / tetrahydrofuran; propan-2-ol / Ambient temperature 4: MnO2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Taguchi, Takeo; Suda, Yoshimitsu; Hosoda, Akihiko; Kobayashi, Yoshiro
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5765 - 5766
反应条件
1: 1.) n-BuLi, 2.) CuI / 1.) THF, -40 deg C, 20 min; 2.) THF, -78 deg C, 2 h 2: 10percent HCl / tetrahydrofuran; propan-2-ol / Ambient temperature 3: MnO2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Taguchi, Takeo; Suda, Yoshimitsu; Hosoda, Akihiko; Kobayashi, Yoshiro
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5765 - 5766
反应条件
1: 10percent HCl / tetrahydrofuran; propan-2-ol / Ambient temperature 2: MnO2 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Taguchi, Takeo; Suda, Yoshimitsu; Hosoda, Akihiko; Kobayashi, Yoshiro
Tetrahedron Letters, 1988 , vol. 29, # 45 p. 5765 - 5766
