119072-55-8合成路线 (共 225 条)
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 7 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 72 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 24 h; Irradiation; Further byproducts given;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 30 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
tert-butylisonitrile in benzene T=20°C; Addition; 72 h; Irradiation; Further byproducts given;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
potassium phosphate; 9-borabicyclo[3.3.1]nonane dimer; tetrakis(triphenylphosphine) palladium(0) 1.) THF, r. t., 2 h, 2.) dioxane, 50 deg C, 6 h; Multistep reaction. Yields of byproduct given;
参考文献
Ishiyama, Tatsuo
Tetrahedron Letters, 1992 , vol. 33, # 31 p. 4465 - 4468
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol Substitution; Heating;
参考文献
Fiumana, Andrea; Jones, Keith
Chemical Communications, 1999 , # 17 p. 1761 - 1762
反应条件
C2H4(P(C6H5)2)2 in dichloromethane Addn. of ligand to CH2Cl2 soln. of complex;; concd. under vac., Et2O was added;;
参考文献
Christofides, Aristides
Inorganica Chimica Acta, 1987 , vol. 133, p. 29 - 32
反应条件
in toluene react. with excess t-C4H9NCO in toluene at room temp.;;
参考文献
Gmelin Handbook: Ni: Org.Verb.1, 1.1.6.4.1, page 327 - 333
反应条件
in toluene room temp.;
参考文献
Gmelin Handbook: Ni: Org.Verb.2, 7, page 393 - 402