119072-55-8合成路线 （共 225 条）
反应条件
Cp'2Nb(H)(η2-C,O-O=C=CPh2) in tetrahydrofuran Ambient temperature;
参考文献
Le, Hoang V.; Ganem, Bruce
Organic Letters, 2011 , vol. 13, # 10 p. 2584 - 2585
反应条件
in chlorobenzene -10°C;
参考文献
Gmelin Handbook: Ni: Org.Verb.2, 7, page 393 - 402
反应条件
1: pyridine With fluorine in dichloromethane T=-78 - -50°C; 2: tert-butylisonitrile in dichloromethane T=-50 - 0°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 46, # 13 p. 2279 - 2282
反应条件
nickel T=170 - 180°C; Hydrogenation;
参考文献
Sabatier; Mailhe
Annales de Chimie (Cachan, France), 1909 , vol. <8>16, p. 107
Full Text Show Details
Sabatier; Mailhe
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1907 , vol. 144, p. 956
Bulletin de la Societe Chimique de France, 1907 , vol. <4>1, p. 614
反应条件
2,2'-azo-bisisobutyronitrile; tris-(trimethylsilyl)silane in toluene T=90°C; 0.5 h;
参考文献
Chatgilialoglu; Giese; Kopping
Tetrahedron Letters, 1990 , vol. 31, # 42 p. 6013 - 6016
反应条件
Yield given. Multistep reaction;
参考文献
Buchwald, Stephen L.; LaMaire, Susan J.
Tetrahedron Letters, 1987 , vol. 28, # 3 p. 295 - 298
反应条件
tetrakis(triphenylphosphine) palladium(0); water; caesium carbonate in acetonitrile T=60°C; 10 h; Inert atmosphere;
参考文献
Zhou, Fengtao; Ding, Ke; Cai, Qian
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12268 - 12271
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene 16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
1: tert-butylisonitrile; 2-Amino-5-fluoro-benzenethiol; hydrochloride in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere; 2: iodobenzene With 1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; palladium diacetate; caesium carbonate in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Bochatay, Valentin N.; Boissarie, Patrick J.; Murphy, John A.; Suckling, Colin J.; Lang, Stuart
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1471 - 1477
反应条件
water; copper diacetate; palladium diacetate; trifluoroacetic acid in tetrahydrofuran T=70°C; 8 h; Sealed tubeAir atmosphere;
参考文献
Peng, Jiangling; Liu, Lanying; Hu, Ziwei; Huang, Jinbo; Zhu, Qiang
Chemical Communications, 2012 , vol. 48, # 31 p. 3772 - 3774
